The milling effect on nickel ferrite particles studied using magnetization measurements and Mössbauer spectroscopy

M. V. Ushakov; M. I. Oshtrakh; A. V. Chukin; V. Šepelák; I. Felner; V. A. Semionkin

doi:10.1007/s10751-017-1478-7

The milling effect on nickel ferrite particles studied using magnetization measurements and Mössbauer spectroscopy

M. V. Ushakov, M. I. Oshtrakh^*, A. V. Chukin, V. Šepelák, I. Felner, V. A. Semionkin

^*Corresponding author for this work

Racah Institute of Physics

Research output: Contribution to journal › Article › peer-review

3 Scopus citations

Abstract

Samples of NiFe₂O₄ nanoparticles N1 (nonactivated), N2 (milled for 15 min) and N3 (milled for 30 min) were studied using X-ray diffraction, scanning electron microscopy with energy dispersion spectroscopy, isothermal magnetization measurement and Mössbauer spectroscopy with respect to analyze the effect of particle milling on their magnetic properties. It was shown that an increase of the milling time lead to: (i) a decrease of particles’ size, (ii) a decrease of the saturation magnetic moment and (iii) an appearance of paramagnetic doublet in the Mössbauer spectra of NiFe₂O₄ nanoparticles.

Original language	English
Article number	4
Journal	Hyperfine Interactions
Volume	239
Issue number	1
DOIs	https://doi.org/10.1007/s10751-017-1478-7
State	Published - 1 Dec 2018

Bibliographical note

Publisher Copyright:
© 2017, Springer International Publishing AG, part of Springer Nature.

Keywords

Hyperfine parameters
Magnetic measurements
Milling effect
Mössbauer spectroscopy
NiFeO nanoparticles

Access to Document

10.1007/s10751-017-1478-7

Cite this

@article{d0288d3011354a57a416385aaec0a1d3,

title = "The milling effect on nickel ferrite particles studied using magnetization measurements and M{\"o}ssbauer spectroscopy",

abstract = "Samples of NiFe2O4 nanoparticles N1 (nonactivated), N2 (milled for 15 min) and N3 (milled for 30 min) were studied using X-ray diffraction, scanning electron microscopy with energy dispersion spectroscopy, isothermal magnetization measurement and M{\"o}ssbauer spectroscopy with respect to analyze the effect of particle milling on their magnetic properties. It was shown that an increase of the milling time lead to: (i) a decrease of particles{\textquoteright} size, (ii) a decrease of the saturation magnetic moment and (iii) an appearance of paramagnetic doublet in the M{\"o}ssbauer spectra of NiFe2O4 nanoparticles.",

keywords = "Hyperfine parameters, Magnetic measurements, Milling effect, M{\"o}ssbauer spectroscopy, NiFeO nanoparticles",

author = "Ushakov, {M. V.} and Oshtrakh, {M. I.} and Chukin, {A. V.} and V. {\v S}epel{\'a}k and I. Felner and Semionkin, {V. A.}",

note = "Publisher Copyright: {\textcopyright} 2017, Springer International Publishing AG, part of Springer Nature.",

year = "2018",

month = dec,

day = "1",

doi = "10.1007/s10751-017-1478-7",

language = "אנגלית",

volume = "239",

journal = "Hyperfine Interactions",

issn = "0304-3843",

publisher = "Springer Nature",

number = "1",

}

TY - JOUR

T1 - The milling effect on nickel ferrite particles studied using magnetization measurements and Mössbauer spectroscopy

AU - Ushakov, M. V.

AU - Oshtrakh, M. I.

AU - Chukin, A. V.

AU - Šepelák, V.

AU - Felner, I.

AU - Semionkin, V. A.

PY - 2018/12/1

Y1 - 2018/12/1

N2 - Samples of NiFe2O4 nanoparticles N1 (nonactivated), N2 (milled for 15 min) and N3 (milled for 30 min) were studied using X-ray diffraction, scanning electron microscopy with energy dispersion spectroscopy, isothermal magnetization measurement and Mössbauer spectroscopy with respect to analyze the effect of particle milling on their magnetic properties. It was shown that an increase of the milling time lead to: (i) a decrease of particles’ size, (ii) a decrease of the saturation magnetic moment and (iii) an appearance of paramagnetic doublet in the Mössbauer spectra of NiFe2O4 nanoparticles.

AB - Samples of NiFe2O4 nanoparticles N1 (nonactivated), N2 (milled for 15 min) and N3 (milled for 30 min) were studied using X-ray diffraction, scanning electron microscopy with energy dispersion spectroscopy, isothermal magnetization measurement and Mössbauer spectroscopy with respect to analyze the effect of particle milling on their magnetic properties. It was shown that an increase of the milling time lead to: (i) a decrease of particles’ size, (ii) a decrease of the saturation magnetic moment and (iii) an appearance of paramagnetic doublet in the Mössbauer spectra of NiFe2O4 nanoparticles.

KW - Hyperfine parameters

KW - Magnetic measurements

KW - Milling effect

KW - Mössbauer spectroscopy

KW - NiFeO nanoparticles

UR - http://www.scopus.com/inward/record.url?scp=85037365678&partnerID=8YFLogxK

U2 - 10.1007/s10751-017-1478-7

DO - 10.1007/s10751-017-1478-7

M3 - ???researchoutput.researchoutputtypes.contributiontojournal.article???

AN - SCOPUS:85037365678

SN - 0304-3843

VL - 239

JO - Hyperfine Interactions

JF - Hyperfine Interactions

IS - 1

M1 - 4

ER -

The milling effect on nickel ferrite particles studied using magnetization measurements and Mössbauer spectroscopy

Abstract

Bibliographical note

Keywords

Access to Document

Other files and links

Fingerprint

Cite this